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The principle reaction of DMDHEU at elevated temperatures in presence of catalyst a variety of acid or latent acid agents with the cellulose is etherification of hydroxyl groups in the amorphous phase causing cross-linking of adjacent cellulose molecules preventing movement of fibre chains under stress thereby hindering wrinkle formation and shrinkage. Tensile and tear strength loss occur due to lack of molecular mobility in cross-links Cooke and Weigmann ; Heywood ; Schindler and Hauser ; Tomasino It is a clear aqueous solution with pH 4—5.

It has high reactivity, extremely low formaldehyde release and is compatible with most of the finishing agents Technical Information Polycarboxylic acids form ester cross-links through esterification reaction with hydroxyl groups of cellulose, in the presence of selective weak catalysts such as alkali metal salts of phosphorous containing inorganic acids, e. Citric acid is the most extensively studied polycarboxylic acid having advantage of being inexpensive, wide availability, non-toxic and environmentally acceptable.

During curing in presence of a catalyst, citric acid forms ester linkage Welch and Peters ; Bhattacharyya et al. The present study was aimed at formulating optimum durable press finish recipe to predict best durable press rating of cotton with two different types of anti-crease chemicals using Box—Behnken designs in conjunction with response surface analysis and regression methods. Thus finished cotton was evaluated for its DP rating followed by various other physical properties too.

Methods Materials Pre-treated plain woven cotton fabric possessing epi: , ppi: 72, warp: 40 s, weft: 40 s and gsm: was used. Statistica 10, Systat 12 and Design Expert 9 softwares were used for sampling as well as analysis of data. Experimental design Box Behnken factorial 63 research designs consisting of 54 runs with six replicates at central point were used to evaluate functional characteristics of modified DMDHEU and citric acid finished cotton. The characteristic of anti-crease finish was evaluated for durable press rating.

Various parameters, viz, concentrations of modified DMDHEU, catalyst, silicone softener SS , polyethylene emulsion PE , curing temperature and time were included in the research design and their levels are mentioned in Table 1. The individual as well as interaction effect of the process factors on durable press rating was examined. Analysis of responses related with independent variables was done using quadratic polynomial equation Eq.

The P values of less than 0. From these runs, sets of runs combinations developing maximum DP rating were selected for further study based on their physical properties. DP rating of control fabric was found to be as poor as 1. However, levels of factors in citric acid finish were subsequently further modified to obtain better DP rating. Magnesium chloride being a latent acid provides stability to the bath and initiates the crosslinking during curing.

Silicone softener reduces strength loss of the fabric. Incorporation of polyethylene emulsion helps in retaining the tear strength properties. Considering DP rating as response dependent variable , the response surface plots are shown in Figs. At resin concentration of 60 gpl along with increased curing temperature i. At lower concentration of catalyst but increase in resin concentration, curing temperature and time did not increase the contribution of magnesium chloride to enhance the DP rating, while, at a higher concentration of it, the increase in resin concentration and curing temperature as well as time increased the effect of magnesium chloride to form more crosslinks with better DP rating Figs.

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